Paramagnetic complexes

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  • The format of this Chapter will be slightly different from that for earlier years. Papers dealing with essentially static situations will be dealt with first – with each Group of the Periodic Table discussed in turn. Results on dynamic systems will then follow – again on the basis of the Periodic Groups, with papers on paramagnetic compounds being dealt with last.

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  • (BQ) Part 2 book "A complete introduction to modern NMR spectroscopy" has contents: The study of dynamic processes by NMR; electron paramagnetic resonance spectroscopy and chemically induced dynamic nuclear polarization; double resonance techniques and complex pulse sequences, two-dimensional nuclear magnetic resonance, NMR studies of biological important molecules,...and other contents.

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  • Ech hydrogenase fromMethanosarcina barkeriis a member of a distinct group of membrane-bound [NiFe] hydrogenases with sequence similarity to energy-conserving NADH:quinone oxidoreductase (complex I). The sequence of the enzyme predicts the binding of three [4Fe-4S] clusters, one by subunit EchC and two by subunit EchF. Previous studies had shown that two of these clusters could be fully reduced under 10 5 Pa of H2at pH 7 giving rise to two distinct S½ electron paramagnetic resonance (EPR) signals, designated as the g¼1.89 and theg¼1.92 signal....

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