Tungsten oxide film was deposited on ITO-coated glass by using RF magnetron sputtering method from WO3 ceramic target. Thin film preparation – process took place in Ar + O2 plasma. The dependence of tungsten oxide film structure on experiment conditions was investigated by X-ray diffraction (XRD) Raman spectroscopy. In this paper, we considered that the thickness of ITO layers about 150nm to 350nm clearly effects on the Raman and XRD spectrograms of WO3 films.
Titanium Silicalite-1 (TS-1) with different contents of titanium were prepared according to the procedure as described in our report . IR, Raman, XRD spectroscopies were used to identify the structure and in-framework, extra-framework titanium ions of TS-1. It is proven that Laser Raman spectroscopy is the most effective method to study the synthesis of TS-1.
Porous hydroxyapatite ceramic was synthesized by solid phase method using Ca(OH)2 and Ca3(PO4)2 at the temperature interval 200 - 350o C. The samples, after pelleting and sintering, were characterized by X-ray diffractometry (XRD), Fourier transform infra-red spectroscopy (FTIR), scanning electron microscopy (SEM) and thermal gravimetric analysis (TGA). Porous structure of hydroxyapatite was obtained with the 42 – 55% porosity.
Wang et al. Nanoscale Research Letters 2011, 6:241 http://www.nanoscalereslett.com/content/6/1/241
High-quality reduced graphene oxidenanocrystalline platinum hybrid materials prepared by simultaneous co-reduction of graphene oxide and chloroplatinic acid
Yinjie Wang, Jincheng Liu*, Lei Liu, Darren Delai Sun*
Abstract Reduced graphene oxide-nanocrystalline platinum (RGO-Pt) hybrid materials were synthesized by simultaneous coreduction of graphene oxide (GO) and chloroplatinic acid with sodium citrate in water at 80°C, of pH 7 and 10.
Titanium oxide ST01, ST31, TiO2 catalysts modified by V5+, N2+ and supported on MCM41 and SiO2 have been used for photooxidation of p-xylene in gas phase. Physicochemical properties of catalysts were determined by the methods of BET Adsorption, Xray Diffraction (XRD), UV-Vis spectroscopy, and atom adsorption spectroscopy (AAS) methods. The photocatalytic activity of catalysts were determined after thermal treatment as well as UV lighting. The common observation is that the higher temperature of treatment the lower conversion of p-xylene obtained.
In this work, platinum nanoparticles were dispersed on SBA-15 mesoporous material by incipient wetness method and the synthesized materials were characterized by XRD, TEM, EDX spectroscopies and N2 adsorption-desorption isotherm measurement. The results indicated that 2D hexagonal ordered structure of SBA-15 was still maintained after grafting Pt on SBA-15 support and platinum nanoparticles existed both inside and outside the pore channels of SBA-15 material. Catalytic activity of these materials was tested in the aqueous phase D-glucose oxidation as a model reaction. ...
The structural, morphological and optical properties of CBD deposited CdS thin films have been studied by varying the processing parameters and the Cd/S ratio of the starting precursors in order to better understand the growth conditions. The films were characterized by Xray diffraction, SEM, Raman, and photoluminescence spectroscopy. XRD patterns show that asdeposited CdS films were polycrystalline. The grain size are increasing with increasing the Cd/S ratio and/or the deposition time.