Electron microscopy

n this work, pectin was extracted from pomelo peel while rice husk ash was used for silica recovery. The obtained CPS were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and Field emission scanning electron microscopy (FE-SEM).

8p viengfa 28-10-2024 1 0   Download

Silver nanoparticles (Ag NPs) were synthesized and characterized by transmission electron microscopy (TEM), X-ray powder diffraction (XRD), and absorption spectroscopy. Using Debye-Scherrer’s formula and the result of the XRD spectrum, the size of the Ag NPs was estimated at approximately 8 nm.

7p viengfa 28-10-2024 0 0   Download

In this paper, ZnO/CuO/Ag ternary composites were successfully synthesized by hydrothermal method using Zn(NO3)2.6H2O, Cu(NO3)2.3H2O and AgNO3. The composite samples were characterized using X-Ray diffraction (XRD), Scanning Electron Microscopy (SEM) and Raman spectroscopy.

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This paper studied the synthesis of calcium oxide (CaO) from snail shells by calcination, crushing, and grinding. Then, the sample was analyzed by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), specific surface area (BET), and particle size.

10p viengfa 28-10-2024 1 1   Download

In this work, ZnFe2O4 nanoparticles were synthesized by hydrothermal method while the hummer method was used to synthesize GO nanosheet. GO/ZnFe2O4 nanocomposites (GO/ZFO) were prepared by mixing GO with ZnFe2O4 in mass ratio of 1:99, respectively.

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In this study, spinel ferrite nanoparticles CoFe2-xLaxO4 (x = 0, 0.025, and 0.05) were successfully synthesized via a simple co-precipitation method using a 5% NaOH solution as a precipitating agent. The physicochemical properties of the materials, annealed at 850 °C for one hour, were characterized using powder X-ray diffraction (PXRD), energy-dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), and vibrating-sample magnetometry (VSM) at room temperature.

10p viling 11-10-2024 1 0   Download

A metal-organic framework Cu2(NDC)2(DABCO) was synthesized from copper nitrate trihydrate, 2,6-Napthalenedicarboxylic acid (H2NDC), and 1,4-diazabicyclo[2.2.2]octane (DABCO) by solvothermal method. Its physicochemical properties were confirmed by several techniques such as X-ray powder diffraction (PXRD), Fourier transform infrared (FT-IR), scanning electron microscopy (SEM), and transmission electron microscopy (TEM).

7p vikwong 29-09-2024 1 0   Download

Bài viết trình bày kết quả nghiên cứu chế tạo vật liệu nano Cu trên bề mặt điện cực indium tin oxide (ITO) bằng phương pháp lắng đọng điện hóa CA (chronoamperometry). Tính chất điện hóa, cấu trúc, hình thái cũng như khả năng xúc tác khử CO2 của các vật liệu được khảo sát bằng các phương pháp quét thế vòng tuần hoàn (cyclic voltammetry – CV), nhiễu xạ tia X (X-ray diffraction - XRD), hiển vi điện tử quét (scanning electron microscopy – SEM) và quét thế tuyến tính (Linear sweep voltammetry – LSV).

5p vikwong 29-09-2024 2 1   Download

In this study, γ-MnOOH nanorods synthesized by polysaccharide- assisted hydrothermal method as an efficient electrocatalyst for urea oxidation. The γMnOOH structure and morphology are confirmed by X-ray diffraction and scanning electron microscopy (SEM).

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A porous crytalline metal-organic framework Fe3O(BPDC)3 was synthesized, and its properties were characterized by various techniques, including X-ray powder diffraction (PXRD), Fourier transform infrared (FT-IR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen physisorption measurements.

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The single phase of Mn0.5Fe2.5O4 spinel crystals was prepared by the microemulsion method with the oil phase is DGDE (diethylene glycol diethyl ether). The characteristics of the materials have been determined by the X-ray diffraction (XRD), Energy-dispersive X-ray spectroscopy (EDX), Scanning electron microscopy (SEM) and Brunaure-Emmet-Teller (BET) nitrogen adsorption and desorption, Vibration sampling magnetometer (VSM), Fourier transform infrared spectroscopy (FTIR).

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The Mn-doped MoS2 (Mn-MoS2) material is fabricated by a facile onestep calcination method. The Mn2+ content introduced into MoS2 is ranged from 1 wt% to 7 wt%. The X-ray diffraction (XRD) and scanning electron microscopy SEM results suggest that the doping of Mn2+ does not alter the crystal structure and the morphology of MoS2.

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In the present work, palladium nanoparticles were synthesized in glycerol following the bottom-up methodology, using Pd(II) and Pd(0) precursors. The as-prepared materials were characterized by transmission electron microscopy (TEM) and powder X-ray diffraction (XRD), evidencing the formation of zerovalent palladium spheres in the nanosize ranges.

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This study investigated adsorption of beta-lactam antibiotic Amoxicillin (AMX) on a new material of cerium oxide-coated nanosilica (CeO2-coated SiO2). The CeO2-coated SiO2 based on rice husk, was characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), and transmission electron microscopy (TEM).

6p vikwong 29-09-2024 2 0   Download

Alginate-stabilized Cu2O@Cu nanoparticles were fabricated by chemical reduction method using nature polymer alginate as a stabilizing agent. Transmission electron microscopy (TEM), X-ray powder diffraction (XRD), infrared (FT-IR) spectrum, and UV-Vis analysis were used to investigate the morphology, size, structure, and stability of the nanoparticles synthesized.

6p vikwong 29-09-2024 4 0   Download

This article reported the preparation of Nano CeO2 by acid method from Binh Dinh monazite ore. Obtained CeO2 was examined by the method of X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM), energy-dispersive X-ray spectroscopy (EDS), specific surface area analysis by Brunauer-Emmet-Teller (BET) method, UVVIS.

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In this study, in-situ method was applied for synthesizing silver-doped graphene oxide (Ag/GO). The material was extensively characterized by X-ray diffraction, Transmission electron microscopy, Scanning electron microscope, Raman spectroscopy, energy-dispersive X-ray spectroscopy, and UV-Vis spectroscopy.

6p vikwong 29-09-2024 3 0   Download

The article will report the purification of Dilinh bentonite sample deposits of Lamdong province in Vietnam. The combination of sonication, sedimentation and dispersant (NaPO3)6 were applied to increase the montmorillonite (MMT) content.

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In this study, the photocatalytic degradation of rhodamine b (RhB) is investigated over metal-organic framework materials based on bismuth and trimesic acid (Bi-BTC) with different metal-to-ligand molar ratios. All obtained products are characterized by using powder X-ray diffraction, scanning electron microscopy, and UV–vis diffuse reflectance spectroscopy.

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The novel composite nanomaterials were synthesized via a simple method from two natural clay mineral sources, graphite and halloysite. The materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FTIR), Brunauer-Emmet-Teller (BET) methods.

10p vikwong 29-09-2024 0 0   Download