Preparation materials

In this study, spinel ferrite nanoparticles CoFe2-xLaxO4 (x = 0, 0.025, and 0.05) were successfully synthesized via a simple co-precipitation method using a 5% NaOH solution as a precipitating agent. The physicochemical properties of the materials, annealed at 850 °C for one hour, were characterized using powder X-ray diffraction (PXRD), energy-dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), and vibrating-sample magnetometry (VSM) at room temperature.

10p viling 11-10-2024 1 0   Download

In this research, we had successfully prepared a series of RF-carbon nitride composites for photocatalyst application. The modification of carbon nitride with RF resins aimed to enhance physical characteristics and photocatalytic activity toward organic pollutants, such as methylene blue. XRD, FTIR, SEM, and N2 adsorptiondesorption isotherms were used to characterize the asprepared composite materials.

10p vikwong 29-09-2024 2 1   Download

This study refers to the preparation of APP/Diatomite (DIA) composite flame-retardant fillers. The materials were prepared by two methods: by adding diatomie powder to the mixture during the preparation of APP or by adding diatomite powder to the suspension of very fine solid APP particals in water.

5p vikwong 29-09-2024 4 1   Download

Porous carbon material is one of the most common and very important for various applications thank to its high surface area and adsorption capability. In this study, mesoporous carbon was prepared by thermal decomposition of copper-based metal-organic framework MOF-199 under inert atmosphere and followed by immersing in diluted HNO3 solution in order to remove metal/metal oxide and activation of the resultant porous carbon.

5p vikwong 29-09-2024 4 1   Download

In this paper, titanium nitride nanofibers (TiN NFs) were successfully synthesized by nitridation of TiO2 nanofibers, in which the TiO2 nanofibers were prepared by using electrospinning method.

6p vikwong 29-09-2024 2 1   Download

The single phase of Mn0.5Fe2.5O4 spinel crystals was prepared by the microemulsion method with the oil phase is DGDE (diethylene glycol diethyl ether). The characteristics of the materials have been determined by the X-ray diffraction (XRD), Energy-dispersive X-ray spectroscopy (EDX), Scanning electron microscopy (SEM) and Brunaure-Emmet-Teller (BET) nitrogen adsorption and desorption, Vibration sampling magnetometer (VSM), Fourier transform infrared spectroscopy (FTIR).

7p vikwong 29-09-2024 3 1   Download

In the present work, palladium nanoparticles were synthesized in glycerol following the bottom-up methodology, using Pd(II) and Pd(0) precursors. The as-prepared materials were characterized by transmission electron microscopy (TEM) and powder X-ray diffraction (XRD), evidencing the formation of zerovalent palladium spheres in the nanosize ranges.

5p vikwong 29-09-2024 3 1   Download

In this study, ZnO was synthesized by the simple hydrothermal method. The physicochemical properties of the materials were characterized by SEM, XRD, N adsorption/desorption isotherm methods.

6p vikwong 29-09-2024 2 1   Download

In this study, graphene oxide (GO) was prepared by the Hummers method. GO/CS/PVA fibers were prepared by an electrospinning method. The structure, morphology and size of the electrospun materials were characterized by X – ray diffraction (XRD) and a scanning electron microscope (SEM).

7p vikwong 29-09-2024 2 1   Download

Non-metallic C, N, and S doped TiO2 materials were prepared using the hydrothermal method from titanyl sulfate solution with different doped precursors. The influence of non-metallic elements on crystal structure, morphology, surface area, bonding state, and light absorption ability of materials was studied through XRD, SEM, BET spectra, and UVis - DRS.

5p vikwong 29-09-2024 3 1   Download

The high durability, re-collectable and low-cost materials with tertiary (reduced graphene-TiO2-Fe3O4, denoted as GrTiFe) components for degradation of toxic organic compounds have been prepared from different precursors by coprecipitation and hydrothermal methods.

5p vikwong 29-09-2024 2 1   Download

Zeolite Socony Mobil-5 (ZSM-5) was successfully synthesized by a hydrothermal method from the silicon dioxide (SiO2) precursor prepared fro m rice husk ash. Titanium dioxide (TiO2) nanoparticles were decorated on ZSM-5 substrate by a sol-gel method. ZSM-5/TiO2 materials were characterized by Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), transmission electron microscope (TEM), and Brunauer-Emmett-Teller (BET) surface area analysis.

6p vikwong 29-09-2024 1 1   Download

In this study, the Cu-TiO2-SBA-16 photocatalytic materials were successfully prepared by direct hydrothermal synthesis method. The products were characterized by X-ray diffraction (XRD), Ultraviolet– Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS), energy dispersive X-ray (EDX), transmission electron microscopy (TEM), N2 adsorption–desorption isotherms, X-ray photoelectron spectroscopy (XPS) methods.

6p vikwong 29-09-2024 3 1   Download

Graphene-based electrode materials exhibit a high specific capacitance and long charge-discharge cycling life, but the material cost remains high because of the complexity of the graphene manufacturing process. This study employed an electrochemical exfoliation method to prepare graphene in a simple and ecologically friendly procedure. According to research findings, the disordered multi-layer structure of graphene exhibited great purity, porosity, and graphitization.

6p vikwong 29-09-2024 2 1   Download

The paper aims to study the effect of operatiing conditions in the column experiment with the ion exchange material which was prepared in optimum synthesized conditions. Polystyrene waste from disposable food packaging was dissolved in cyclohexane and sulfonated by sulfuric acid to synthesize cation exchange materials which were applied to remove Cr3+ in water by the ion exchange principle.

9p viyoko 24-09-2024 2 1   Download

The process of mechanical root canal preparation creates smear layer. The smear layer can prevent the penetration of intracanal medicaments into dentinal tubules and influence the adaptation of filling materials to canal walls. The purpose of this study is to compare the smear layer removal ability of root canal irrigation methods with chelat solution.

6p vifaye 20-09-2024 2 1   Download

In this study, a thermosetting benzoxazine was successfully prepared from environmentally friendly sources to be used as an adhesive. The phenolic component used for the synthesis of the benzoxazine monomer is cardanol derived from the cashew nutshell, while the amine fractions are terephthalamide, which is a product of the amination process of used polyethylene terephthalate plastic bottles (PET).

11p xuanphongdacy06 18-09-2024 3 1   Download

In this work, SrFe12O19 samples were synthesized by hydrothermal method. We systematically studied the influence of an alkaline environment (NaOH) with the molar ratio (R) of 2 , 3 and 4 on the structure, magnetic properties of SrFe12O19 particles prepared by hydrothermal method. The relation between morphology, magnetic properties and microwave absorption properties of materials have been investigated.

8p viambani 18-06-2024 2 1   Download

The specific objectives of this study are: 1. To conduct a literature review on carbon-based hydrogen storage electrodes and direct proton absorbance in various forms of carbon; 2. To prepare and characterise activated carbon samples with proper porosity for the present application; 3. To manufacture and characterise a range of composite materials containing carbon material and a proton-conducting medium such as nafion in various levels of hydration 4. To fabricate a number of membrane-electrode-assembly (MEA) from the composite materials;…

264p runthenight05 01-03-2023 6 3   Download

The focus of this study is to investigate its optical and conductive properties under different conditions of doping environments, temperature and polymerization conditions. Optical characterization technique such as UV-Visible spectroscopy is developed to carry out the investigation. The developed nanofibers have been demonstrated to possess optical and conductive properties to be dependent on doping variables. Study of these optical properties could prove very useful in the development of electrochromic devices and gas sensors.

103p runthenight07 01-03-2023 7 3   Download