Synthesis structural and electrochemical properties

This study aims to investigate the effectiveness of the green microwave technique in producing 1T/2H-MoS2 nanomaterials using polyol solvents. The paper presents a thorough analysis of the structural and property characteristics of the synthesized materials and elucidates the underlying chemical mechanism that governs the formation of hybrid-phase nanostructures. Additionally, the role of polyol solvents in the practical synthesis of nano MoS2 under microwave heating is evaluated and explained.

15p xuanphongdacy06 18-09-2024 1 1   Download

These results indicate that sol-gel processing is a promising method for preparing Ni-rich cathode materials. The sample prepared under the optimal conditions had a well ordered hexagonal layered structure. The charge–discharge tests showed that the initial capacities of the sample were 220.456 and 185.937 mAhg -1 at the discharge rate of 0.1 C between 3.0 and 4.3 V, respectively. The capacity retention ratio was 81.36 % at 1 C after 50 cycles.

5p lamtan3547 04-11-2018 20 0   Download

The oxide reduction diffusion (ORD) procedure has recently been applied in synthesizing hydrogen storage materials AB5 for Ni-MH batteries. Starting from metal hydroxides and La oxalat precursor, superfine powder alloys LaNi5, LaNi4.5Co0.5 and LaNi3.87Mn1.13 were obtained by this “soft-chemistry” route. Chemical composition, structure and morphology of alloy phases were examined by different analysis techniques such as AAS, EPMA, X-ray and TEM. The H2-absorption and desorption behavior of crystalline products was determined by Sieverts’ method.

9p uocvong01 24-09-2015 37 3   Download