Crystal x-ray diffraction

Iron oxide nanorods were synthesized by chemical co-precipitation method. The structural and morphological characteristics of the as-synthesized nanorods were analyzed by Xray diffraction (XRD) and scanning electron microscopy. The results show that the iron oxide nanorods include the mixture of Fe3O4, γ-Fe2O3 and FeOOH with the diameter and the length of iron oxide nanorods to be 30 and 100 nm, respectively. The iron oxide nanorods were then dispersed and deposited on the gold electrode of quartz crystal microbalance (QCM) for the gas sensor.

8p nguyenminhlong19 22-04-2020 30 1   Download

In this report, thin layers of MoS2 were in-situ incorporated into graphene oxide (GO) to form MoS2/graphene nanocomposite by a facile ultrasonic-assisted hydrothermal method. Xray Diffraction (XRD) and Raman analysis revealed that the as-synthesized MoS2 nanosheets crystalized in hexagonal phase 2H-MoS2 while High Resolution Transmission Electron Microscopy (HRTEM) images confirmed that MoS2 layers with average thickness of ~5–6 nm (6–8 layers) attached on the edges and surfaces of graphene sheets with high density and uniform shape restacking in three-dimensional (3D) architectures.

11p chauchaungayxua2 07-01-2020 28 0   Download

The N,O-bidentate ligand 2-((methylimino)methyl)pyren-1-ol (1) gives with nickel acetate in a mixed solvent of toluene and ethanol in the presence of NaOAc the nickel(II) complex 1(Ni). It was characterized by elemental analysis, IR, NMR, MS spectroscopy and single crystal Xray diffraction. With respect to the nickel atom the complex 1(Ni) adopts a distorted square planar trans-coordination geometry.

8p cathydoll4 21-02-2019 24 0   Download