Fourier transforms infrared

n this work, pectin was extracted from pomelo peel while rice husk ash was used for silica recovery. The obtained CPS were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and Field emission scanning electron microscopy (FE-SEM).

8p viengfa 28-10-2024 2 0   Download

This paper studied the synthesis of calcium oxide (CaO) from snail shells by calcination, crushing, and grinding. Then, the sample was analyzed by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), specific surface area (BET), and particle size.

10p viengfa 28-10-2024 1 1   Download

In this work, ZnFe2O4 nanoparticles were synthesized by hydrothermal method while the hummer method was used to synthesize GO nanosheet. GO/ZnFe2O4 nanocomposites (GO/ZFO) were prepared by mixing GO with ZnFe2O4 in mass ratio of 1:99, respectively.

8p viengfa 28-10-2024 3 1   Download

A metal-organic framework Cu2(NDC)2(DABCO) was synthesized from copper nitrate trihydrate, 2,6-Napthalenedicarboxylic acid (H2NDC), and 1,4-diazabicyclo[2.2.2]octane (DABCO) by solvothermal method. Its physicochemical properties were confirmed by several techniques such as X-ray powder diffraction (PXRD), Fourier transform infrared (FT-IR), scanning electron microscopy (SEM), and transmission electron microscopy (TEM).

7p vikwong 29-09-2024 2 1   Download

The aim of this study was to design and characterize a NdFeO3-based photocatalyst prepared by sol-gel method for treatment of oily wastewater. Different characterization techniques such as X-ray diffraction (XRD), scanning electron microscope (SEM), Fourier transform infrared spectroscopy (FTIR), UV–vis spectrophometer were used to elucidate the structure, morphology, surface functional groups, and optical absorption properties of the prepared NdFeO3 photocatalyst.

6p vikwong 29-09-2024 2 1   Download

Reduced graphene oxide (Gr) has been synthesized electrochemically on the surface of copper metal at a fixed potential of 1.5 V versus a standard saturated calomel electrode (SCE). The synthesized Gr was then characterized with X-Ray diffraction, thermogravimetric analysis, raman and Fourier transform infrared (FT-IR) spectroscopies.

6p vikwong 29-09-2024 3 1   Download

A porous crytalline metal-organic framework Fe3O(BPDC)3 was synthesized, and its properties were characterized by various techniques, including X-ray powder diffraction (PXRD), Fourier transform infrared (FT-IR), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and nitrogen physisorption measurements.

8p vikwong 29-09-2024 5 1   Download

The single phase of Mn0.5Fe2.5O4 spinel crystals was prepared by the microemulsion method with the oil phase is DGDE (diethylene glycol diethyl ether). The characteristics of the materials have been determined by the X-ray diffraction (XRD), Energy-dispersive X-ray spectroscopy (EDX), Scanning electron microscopy (SEM) and Brunaure-Emmet-Teller (BET) nitrogen adsorption and desorption, Vibration sampling magnetometer (VSM), Fourier transform infrared spectroscopy (FTIR).

7p vikwong 29-09-2024 3 1   Download

This study investigated adsorption of beta-lactam antibiotic Amoxicillin (AMX) on a new material of cerium oxide-coated nanosilica (CeO2-coated SiO2). The CeO2-coated SiO2 based on rice husk, was characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), and transmission electron microscopy (TEM).

6p vikwong 29-09-2024 3 1   Download

The novel composite nanomaterials were synthesized via a simple method from two natural clay mineral sources, graphite and halloysite. The materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FTIR), Brunauer-Emmet-Teller (BET) methods.

10p vikwong 29-09-2024 1 1   Download

Zeolite Socony Mobil-5 (ZSM-5) was successfully synthesized by a hydrothermal method from the silicon dioxide (SiO2) precursor prepared fro m rice husk ash. Titanium dioxide (TiO2) nanoparticles were decorated on ZSM-5 substrate by a sol-gel method. ZSM-5/TiO2 materials were characterized by Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), transmission electron microscope (TEM), and Brunauer-Emmett-Teller (BET) surface area analysis.

6p vikwong 29-09-2024 1 1   Download

The characterization and morphology of chitosan beads were investigated by Fourier-transform infrared spectroscopy technique (FT-IR), optical microscope and scanning electron microscope technique (SEM). The influence of NaOH concentration, pH, reaction time and adsorption isotherm was studied.

6p vikwong 29-09-2024 3 1   Download

A series of Mg-Cu-Al hydrotalcite/chitosan materials have been synthesized via a co-precipitation method, in which chitosan is synthesized from chitin extraction from waste shrimp shells. The obtained solids were characterized by XRD, BET, EDX, IR techniques. The materials have a well crystallized hydrotalcite structure and medium surface area.

5p vikwong 29-09-2024 3 1   Download

Mesoporous silica nanoparticles (MSNs) have been used as an anticancer drug delivery system with high safety and entrapment capacity thanks to their large internal space for drug accommodation, durable structure, and good biocompatibility. However, the treatment efficiency of the bare MSNs is limited due to its drug leakage and burst release. In this study, a phospholipid bilayer was covered on the MSNs surface (MSN@Lip) as a liposomal cap that not only reduced drug leakage but also improved the stability of the colloidal system.

8p dianmotminh02 03-05-2024 7 1   Download

Nano-hydroxyapatite/starch composite was synthesized using in situ precipitation. Starch concentration effect on the structure of composite was examined. Characterization of the obtained samples, The X-ray diffraction and Fourier transform infrared spectroscopy demonstrated the purity of the formed nano-HA in the starch matrix. Morphology studies of the samples, checked by field emission scanning electron microscope and transmission electron microscope, show the effects of starch on the size, shape, and morphology of hydroxyapatite nanoparticles.

6p dianmotminh02 03-05-2024 7 2   Download

The 3D printing PMMA/ZrO2 filaments with a diameter of 1.75±0.05 mm were fabricated by using a single-screw extruder at temperatures of four heating zones of 190, 200, 210, and 210°C. Testing samples were prepared from the extruded filaments by using a fusion deposition modeling 3D printer and a Haake MiniJet piston injection molding machine. Fourier transform infrared spectroscopy, mechanical properties, field emission scanning electron microscopy (FESEM), differential scanning calorimetry, and thermogravimetric analysis of the filaments were investigated.

9p dianmotminh02 03-05-2024 2 1   Download

In the present study, a complex between 8-hydroxyquinoline and cerium (III) (CeHQ) was synthesized in the presence of triethylamine. Afterwards, the complex was characterized by Field Emission Scanning Electron Microscopy (FESEM), Fourier-transform infrared spectroscopy (FTIR) and Thermo-Gravimetric Analysis (TGA). The inhibition efficiency of the Ce-HQ complex for the corrosion of carbon steel, evaluated by both Electrochemical Impedance Spectroscopy (EIS) and Potentiodynamic Polarization (PP) plots, reached 90 % after 2 h of immersion in a 0.01 M NaCl solution.

13p dianmotminh02 03-05-2024 6 2   Download

Petrified wood samples are found within terrestrial sediments belonging to the Late Oligocene-Early Miocene Danişmen Formation in Malkara-Keşan located in the southwest of the Thrace Basin. The petrified wood in both regions is usually silicified and partly coalified. The silicification of the Tertiary wood in the Malkara-Keşan region is associated with volcanic activity and coeval sedimentation. Thin sections from petrified wood samples were taken as transverse, tangential, and radial sections.

22p tanmocphong 29-01-2022 24 1   Download

Borotellurite glasses were prepared by melt quenching technique. Amorphous nature of samples was confirmed through X-ray diffraction (XRD) patterns. Effect of B2O3 content on the structure of glass network was studied through Fourier-transform infrared spectroscopy (FTIR) spectra. Optical band gap and Urbach energy were found from analysis of optical absorption spectra. Thermal studies were carried out by using Differential thermal analyzer (DTA) measurements.

8p tamynhan6 14-09-2020 14 2   Download

The experimental results show that the highest photocatalytic activity was obtained from the Ag (5) doped Zn-0.75Al-0.25La-CO3 photocatalysts calcined at 500 0C with a degradation efficiency of 99,4 after 40 min of irradiation only. This study could provide a new route for the fabrication of high performance photocatalysts and facilitate their application in the environmental remediation issues.

13p tamynhan4 06-09-2020 10 3   Download