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Nuclear magnetic resonance

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  • Lecture Organic chemistry - Chapter 10: Nuclear magnetic resonance (NMR) spectroscopy. In this chapter, the following content will be discussed: What is spectroscopy? General spectrometer, the chemical shift δ, complex splitting patterns,...and other contents.

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  • NMR is an experiment in which the resonance frequencies of nuclear magnetic systems are investigated. NMR always employs some form of magnetic field (usually a strong externally applied field B0) NMR is a form of both absorption and emission spectroscopy, in which resonant radiation is absorbed by an ensemble of nuclei in a sample, a process causing detectable emissions via a magnetically induced electromotive force.

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  • The Biological Magnetic Resonance Data Bank (BMRB) is a public repository of Nuclear Magnetic Resonance (NMR) spectroscopic data of biological macromolecules. It is an important resource for many researchers using NMR to study structural, biophysical, and biochemical properties of biological macromolecules.

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  • Since its first implementation by Lauterbur [1], Magnetic Resonance Imaging (MRI) has become an important noninvasive imaging modality. MRI has found a number of applications in the fields of biology, engineering, and material science. Because it provides unique contrast between soft tissues (which is generally superior to that of CT) and high spatial resolution, MRI has revolutionized diagnostic imaging in medical science. An important advantage of diagnostic MRI as compared to CT is that the former does not use ionizing radiation....

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  •  NMR in solids, like solution-state, relies on the behavior of nuclear spin energy levels in a magnetic field. However, the interactions that affect NMR spectra act differently.  In liquids, molecules reorient and diffuse quickly, leading to narrow isotropic resonances.  In solids, the fixed orientation of individual crystallites leads to a range of resonance frequencies for anisotropic interactions.

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  • (bq) part 1 book "introduction to spectroscopy" has contents: molecular formulas and what can be learned from them, infrared spectroscopy, nuclear magnetic resonance spectroscopy, nuclear magnetic resonance spectroscopy,,...and other contents.

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  • (bq) part 2 book "introduction to spectroscopy" has contents: ultraviolet spectroscopy, mass spectrometry, combined structure problems, nuclear magnetic resonance spectroscopy.

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  • Acta Veterinaria Scandinavica Research Tuyển tập các báo cáo nghiên cứu về bệnh học thý y được đăng trên tạp chí Acta Veterinaria Scandinavica cung cấp cho các bạn kiến thức về bệnh thú y đề tài: Proton nuclear magnetic resonance spectroscopy based investigation on propylene glycol toxicosis in a Holstein cow...

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  • (bq) part 1 book "organic chemistry principles in context" has contents: from cellulose and starch to the principles of structure and stereochemistry, a survey of the experiments usually performed by chemists to understand the structures of organic molecules - mass spectrometers, infrared spectrometers and nuclear magnetic resonance spectrometers,...and other contents.

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  • Chapter 13 - Nuclear magnetic resonance spectroscopy. In this chapter, students will be able to understand: Use the chemical shifts, splitting patterns, and integrations shown in a proton NMR spectrum to propose structures for possible compounds; use the number of peaks and their chemical shifts in a 13C NMR spectrum to determine the number of types of carbon atoms in the compound and what functional groups they might represent;...

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  • A new monomer of N-benzoyl dithieno[2,3- b:2’,3’-d]pyrrole (BDP), has been successfully prepared via copper-catalyzed amidation. Then, this monomer was brominated to form 2,6- dibromo-n-benzoyl dithieno[2,3-b:2’,3’- d]pyrrole (DiBDP) monomer. The structures of monomers were confirmed via the nuclear magnetic resonance (1HNMR) and Fourier transform infrared (FT-IR). BDP and DiBDP monomers will be used as monomers for Suzuki polycondensation reaction to synthesize the donor-acceptor (D-A) conjugated polymers.

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  • The typical synthesis procedure for the monomer of N,N-diphenyl-4-vinylaniline was conducted and has been proved to be ineffective in the university laboratory conditions. The modified procedure was applied successfully using freshly formed Wittig reagent. The monomer was characterized by proton nuclear magnetic resonance (1H NMR) spectroscopy and confirmed the chemical structure with the correct peaks. The photoconductive polymer of poly((4- diphenylamino styrene)) could be obtained only by using the white crystal monomer.

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  • In this study, the synthesis of a telechelic linker bearing both azide and thiol functional groups was described. The reaction conditions were investigated to optimize the reaction yield. The product was analyzed using thin layer chromatography (TLC) and proton nuclear magnetic resonance (1 H NMR).

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  • The resulting TE-NRs were characterized by nuclear magnetic resonance (NMR) spectroscopy, Fourier transform infrared (FT-IR) spectroscopy and size exclusion chromatography (SEC). Epoxy group was found for PC, STR5L, RSS3, TSS8® and SMR20 and trans-1,4-isoprene unit from trans-1,4-isoprene units from cis-trans isomerization was found for TSS8® and SMR20 from the assignments of 1H-NMR signals.

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  • The purpose of this study is to synthesize and characterize poly (ethylene glycol) methyl ether (mPEG) conjugated chitosan (CS), mPEG-CS, at different ratios of 5-Fluorouracil (5-FU) delivery (5-FU-loaded mPEG-CS). The chemical cross-linking of these polymers were prepared by using 4-Nitrophenyl chloroformate reagent. The obtained mPEG-CS was characterized by Fourier transform infrared (FTIR) and proton nuclear magnetic resonance (1H NMR) spectroscopy.

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  • Today, most investigations of the plant metabolome tend to be based on either nuclear magnetic resonance (NMR) spectroscopy or mass spectrometry (MS), with or without hyphenation with chromatography. Although less sensitive than MS, NMR provides a powerful complementary technique for the identification and quantification of metabolites in plant extracts.

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  • In the previous study, a new method was established to prepare mannan under mild conditions by using antibiotic Benanomicin A. In this study, this method was applied to the isolation of P. pastoris NBRC 0984 mannan which predominantly contains β-1,2- linked mannose residues.

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  • The three derivatives of 2-pyrrolidinone were synthesized based on a multi-component reaction, using an eco-friendly solvent, ethanol. Some of the advantages of a multi-component reaction are the simple way of conducting experiments, using low-cost and fairly common materials. Besides, the structure of these three compounds is explained based on spectral methods such as infrared (IR), mass spectrometry (MS) and nuclear magnetic resonance (NMR).

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  • In this work, we studied the applicability of diffusion ordered nuclear magnetic resonance spectroscopy (DOSY NMR) as an alternative method in determination of polystyrene molecular weight. DOSY NMR spectroscopy allows measuring the diffusion coefficient of molecule which directly depend on hydrodynamic radius and so on, average molar mass in weight (Mw).

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  • The aim of this work was to develop and validate the ES qNMR method based on PULCON principle using ERETIC-2 tool to determine concentration and purity of organic compounds through the testing of two certified reference materials (CRMs) and three highly interested chemical pharmaceutical materials (CPM) extracted in Viet Nam, thereby establishing procedure for PULCON based ES qNMR method and assessing the applicability of this potential and promising analysis method for the analysis of Vietnamese medicinal herbs.

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