Electrochemical method

In this work, the electrochemical behavior of lead has been investigated with sensitive, fast and simple different pulse anodic stripping voltammetry (DPASV) method. This preliminary work is an initial step toward the fabricating one type of electrochemical sensors used for sensitive determination of Pb (II) at trace concentration.

8p viyoko 01-10-2024 4 1   Download

This research aims to synthesize MoS2 thin film for the hydrogen evolution reaction (HER) by the electrochemical way. We investigated various electrochemical conditions, including the pH of electrolyte, the applied current density, and electrolysis time to find optimal synthesis mode.

7p vikwong 29-09-2024 2 2   Download

Graphene-based electrode materials exhibit a high specific capacitance and long charge-discharge cycling life, but the material cost remains high because of the complexity of the graphene manufacturing process. This study employed an electrochemical exfoliation method to prepare graphene in a simple and ecologically friendly procedure. According to research findings, the disordered multi-layer structure of graphene exhibited great purity, porosity, and graphitization.

6p vikwong 29-09-2024 3 1   Download

This study presents a preliminary investigation on using pristine aluminum particles as anodes for lithium-ion battery. The microstructural characteristics of aluminum particle samples with sizes from 100 nm (0.1 μm) to 70 µm were analyzed by the SEM and XRD methods. The electrochemical behaviors of the aluminum particles were examined by the cyclic voltammetry (CV) and galvanostatic charge/discharge (GCD) measurements.

7p vikwong 29-09-2024 2 1   Download

This study investigated experimental bearing capacity of corroded reinforced concrete beams. Six testing beams were made of concrete having compressive strength of 25 MPa, with the dimensions of 80 x 120 x 1200 mm. They were divided into two groups depending of tension reinforcement ratio.

11p viyoko 24-09-2024 3 1   Download

The present study focuses on the preparation of silver/copper bimetallic hybrid nanoparticles by green method from precursor solutions of silver nitrate & copper nitrate and the locally available citrus fruit (lemon) peel extract which behaves as the stabilizing and reducing agent. Initially, the formation of hybrid nanoparticles was noticed in the reaction mixture by colour change.

7p dianmotminh02 03-05-2024 7 2   Download

In the paper "Experimental and theoretical studies on the composite composed of graphene oxide and polyaniline", we report theoretical and experimental results on graphene oxide – polyaniline composites. Experimental results in this study were obtained by using different techniques: X-ray diffraction (XRD), Scanning electron microscope (SEM) and from cyclic voltammetry. The theoretical results were acquired using method of density functional theory (DFT).

5p runordie3 27-06-2022 14 3   Download

In this thesis, I have developed a low-cost, simple and one-step approach to synthesize MnO2/graphene composite with enhanced electrochemical performance. MnO2/graphene composite was prepared via a plasma-assisted electrochemical exfoliation method with an electrolyte solution made of KMnO4 precursor.

60p closefriend03 13-10-2021 13 2   Download

In this thesis, we research and fabricate AgNDs, AgNFs, AuNFs structures on silicon by chemical deposition and electrochemical deposition method for the main purpose of using as SERS substrate. To this target, we have studied the morphology, structure and some properties of the nanostructures produced.

26p extraenglish 24-05-2021 26 4   Download

In this thesis, we research and fabricate AgNDs, AgNFs, AuNFs structures on silicon by chemical deposition and electrochemical deposition method for the main purpose of using as SERS substrate. To this target, we have studied the morphology, structure and some properties of the nanostructures produced.

26p capheviahe27 23-02-2021 33 4   Download

In this work, nanoscale bimetallic PtNi, PtCo, PtCu catalysts on carbon Vulcan XC72R as supports were synthesized by reduction method under ultrasonic irradiation. The morphology, structure and specific area of synthesized materials were characterized by X-Ray diffraction (XRD), transmission electron microscopy (TEM). The catalytic activity for oxygen reduction reaction (ORR) of PtM/C was investigated by CV and linear sweep voltammetry (LSV) under simulated fuel cell working conditions.

8p abcxyz123_02 03-03-2020 9 1   Download

The objectives of the thesis: Research and fabricate the one-dimensional (1D) – nanoporous silicon microcavity (1D-NPSMC) structures by using electrochemical etching method with the selectivity of wavelength in visible range from 200 nm to 800 nm.

28p xacxuoc4321 09-07-2019 30 5   Download

The objectives of the thesis: Research and fabricate the one-dimensional (1D) – nanoporous silicon microcavity (1D-NPSMC) structures by using electrochemical etching method with the selectivity of wavelength in visible range from 200 nm to 800 nm. The 1D-NPSMC structures has high reflectivity, narrow linewidth of the pass-band and homogeneous pores.

28p xacxuoc4321 09-07-2019 42 6   Download

These results indicate that sol-gel processing is a promising method for preparing Ni-rich cathode materials. The sample prepared under the optimal conditions had a well ordered hexagonal layered structure. The charge–discharge tests showed that the initial capacities of the sample were 220.456 and 185.937 mAhg -1 at the discharge rate of 0.1 C between 3.0 and 4.3 V, respectively. The capacity retention ratio was 81.36 % at 1 C after 50 cycles.

5p lamtan3547 04-11-2018 20 0   Download

In this paper, Ni - SiC composite coatings were deposited by conventional electroplating from sulfate-chloride bath, and brush electroplating methods from modified chloride bath with different dispersed SiC contents. The plating conditions were investigated and the process’ parameters were defined through electrochemical technique.

9p tieuthi3006 16-03-2018 25 0   Download

The corrosion rate of the CT3 steel in 1 N and 2 N hydrochloric acids was measured by electrochemical polalization method. The measuring values of icorrosion showed that alcoholoamines influence on the inhibition corrosion of the CT3 steel in the hydrochloric acid solution and these values are increased in the order: monoethanolamine < diethanolamine < triethanolamine. In the solution of HCl 1 N and 2 N, the inhibition on the corrosion of steel CT3 of mixture of alcoholamines and potassium iodide is more effective than partial components.

5p uocvong04 24-09-2015 59 5   Download

Effect of sodium nitrite on the carbon steel corrosion inhibition in the aerated neutral (pH 7) and alkaline (pH 11) water solutions at temperatures from 30o C to 140o C has been investigated by mass loss, potentiodynamic polarization and electrochemical impedance spectroscopy methods. Sodium nitrite was added in concentrations: 200, 350, 500, 750, 1000, 1500 and 2000 ppm by mass.

6p uocvong04 24-09-2015 34 4   Download

The conducting polymer poly(5-hydroxy-1,4-naphthoquinone-co-5-hydroxy-3-acetic acid-1,4- naphthoquinone) with electroactive quinone group was investigated by Electrochemical Impedance Spectroscopy (EIS) in aqueous medium. The evaluations of parameters of equivalent circuit in term of applied potential were considered. The simulated EIS data presented a good agreement with the results obtained by other electrochemical methods.

5p uocvong03 24-09-2015 63 3   Download

Inhibition ability of mild steel corrosion of 4 amides (RCONH2 (marked as A4), RCONH– CH2–CH2OH (marked as A5), RCON(CH2–CH2OH)2 (marked as 6b) and RCONH–(CH2)2–NH– COR (marked as 7c) prepared as derivatives from aliphatic acid oxidatively synthesized from nparaffin of Vietnam crude oil, has been examined by electrochemical methods. The corrosion test has been performed in chloride 3% solution at room temperature. The inhibition efficiency has been evaluated through corrosion potential Ecor, corrosion current icor and some other corrosion parameters.

4p uocvong02 24-09-2015 52 3   Download

The oxide reduction diffusion (ORD) procedure has recently been applied in synthesizing hydrogen storage materials AB5 for Ni-MH batteries. Starting from metal hydroxides and La oxalat precursor, superfine powder alloys LaNi5, LaNi4.5Co0.5 and LaNi3.87Mn1.13 were obtained by this “soft-chemistry” route. Chemical composition, structure and morphology of alloy phases were examined by different analysis techniques such as AAS, EPMA, X-ray and TEM. The H2-absorption and desorption behavior of crystalline products was determined by Sieverts’ method.

9p uocvong01 24-09-2015 37 3   Download