Electrochemical synthesis

Reduced graphene oxide (Gr) has been synthesized electrochemically on the surface of copper metal at a fixed potential of 1.5 V versus a standard saturated calomel electrode (SCE). The synthesized Gr was then characterized with X-Ray diffraction, thermogravimetric analysis, raman and Fourier transform infrared (FT-IR) spectroscopies.

6p vikwong 29-09-2024 3 1   Download

In this study, a layered O3-type Ni-rich cathode material for sodium-ion batteries was synthesized through co-precipitation followed by a solid-state reaction at 650 oC in dry air. The electrochemical properties of the Ni-rich material were evaluated. Charge/discharge performance demonstrated that the material delivered higher capacity compared to other layered oxides.

6p vikwong 29-09-2024 2 1   Download

This research aims to synthesize MoS2 thin film for the hydrogen evolution reaction (HER) by the electrochemical way. We investigated various electrochemical conditions, including the pH of electrolyte, the applied current density, and electrolysis time to find optimal synthesis mode.

7p vikwong 29-09-2024 2 2   Download

Graphene-based electrode materials exhibit a high specific capacitance and long charge-discharge cycling life, but the material cost remains high because of the complexity of the graphene manufacturing process. This study employed an electrochemical exfoliation method to prepare graphene in a simple and ecologically friendly procedure. According to research findings, the disordered multi-layer structure of graphene exhibited great purity, porosity, and graphitization.

6p vikwong 29-09-2024 3 1   Download

This study aims to investigate the effectiveness of the green microwave technique in producing 1T/2H-MoS2 nanomaterials using polyol solvents. The paper presents a thorough analysis of the structural and property characteristics of the synthesized materials and elucidates the underlying chemical mechanism that governs the formation of hybrid-phase nanostructures. Additionally, the role of polyol solvents in the practical synthesis of nano MoS2 under microwave heating is evaluated and explained.

15p xuanphongdacy06 18-09-2024 1 1   Download

The present study focuses on the preparation of silver/copper bimetallic hybrid nanoparticles by green method from precursor solutions of silver nitrate & copper nitrate and the locally available citrus fruit (lemon) peel extract which behaves as the stabilizing and reducing agent. Initially, the formation of hybrid nanoparticles was noticed in the reaction mixture by colour change.

7p dianmotminh02 03-05-2024 7 2   Download

Nanocomposite material LiFe1-xMxPO4/Gr was successfully synthesized achieving it with single phase. It’s response required electrochemical parameters of positive electrode materials for Li-ion batteries such as: improved diffusion coefficient and conductivity, higher capacity comparative with LFP in same conditional synthesis.

28p capheviahe26 25-01-2021 21 3   Download

These results indicate that sol-gel processing is a promising method for preparing Ni-rich cathode materials. The sample prepared under the optimal conditions had a well ordered hexagonal layered structure. The charge–discharge tests showed that the initial capacities of the sample were 220.456 and 185.937 mAhg -1 at the discharge rate of 0.1 C between 3.0 and 4.3 V, respectively. The capacity retention ratio was 81.36 % at 1 C after 50 cycles.

5p lamtan3547 04-11-2018 20 0   Download

This study is focused on the synthesis of a polyindole doped by indole-3 butyric acid (PI-IBA). IR analyze indicated that the linkage positions of indole involves the position 2 and 3 of the monomer and the insertion of IBA in the polymer backbone. Polyindole IBA doped was incorporated into epoxy resin for protection anticorrosion of carbon steel. The electrochemical impedance measurements show a significantly improvement of protective properties in presence of PI-IBA in comparison with pure epoxy and epoxy containing polyindole coating.

6p uocvong01 24-09-2015 49 4   Download

The oxide reduction diffusion (ORD) procedure has recently been applied in synthesizing hydrogen storage materials AB5 for Ni-MH batteries. Starting from metal hydroxides and La oxalat precursor, superfine powder alloys LaNi5, LaNi4.5Co0.5 and LaNi3.87Mn1.13 were obtained by this “soft-chemistry” route. Chemical composition, structure and morphology of alloy phases were examined by different analysis techniques such as AAS, EPMA, X-ray and TEM. The H2-absorption and desorption behavior of crystalline products was determined by Sieverts’ method.

9p uocvong01 24-09-2015 37 3   Download

The synthesis and involvement of H2O2 during the early stages of melano-genesis involving the oxidations of DOPA and dopamine (diphenolase activity) were established by two sensitive and specific electrochemical detection systems. Catalase-treated reaction mixtures showed diminished rates of H2O2 production during the autoxidation and tyrosinase-mediated oxidation of both diphenols.

0p awards 06-04-2013 32 3   Download