Forming limit curve determination

In the present work, a simple automated microplate method based on cupric ion reduction is described for determining total reducing sugars in food extracts and synthetic serum. The reaction of Cu(II)-Nc (cupric-neocuproine) with reducing sugars was performed in alkaline medium in microplates, and the absorbance of the formed highly colored Cu(I)-Nc chelate in a plate reader at 450 nm was recorded. The proposed method was applied to reducing sugars (glucose, fructose, galactose, maltose, and lactose) and their linear calibration curves were constructed.

14p tudichquannguyet 29-11-2021 11 1   Download

A novel simple, direct and selective gas chromatography–mass spectrometry (GC/MS) procedure was developed for the determination of the antihistamine drug dimenhydrinate (DMH) in presence of six of its related substances and potential impurities, namely, diphenylmethane, diphenylmethanol, benzophenone, orphenadrine, caffeine and 8-chlorocaffeine. The method involved resolution of the underivatized compounds using a trifluoropropylmethyl polysiloxane (Rtx-200) capillary column and the mass spectrometric detection was carried out in the electronimpact (EI) mode.

6p kequaidan1 16-11-2019 16 0   Download

In this paper, the FLC of the AA6061-T6 aluminum alloy sheet is predicted by using a micro-mechanistic constitutive model. The proposed constitutive model is implemented via a vectorized user-defined material subroutine (VUMAT) and integrated with finite element code in ABAQUS/Explicit software.

10p miulovesmile2 01-11-2018 19 1   Download

This paper contains experimental results for mechanical characteristics of a mild steel sheet. The determination of the forming limit stress curve for solicitation along two direction is drawn. Study of prestrain influence from the limit stress diagram is presented.

8p chikychiky 27-10-2018 35 1   Download