Hydrothermal synthesis

In this study, we report on the hydrothermal synthesis of ZnO nanorods and the change in photocatalytic properties with different hydrothermal temperatures in the decomposition of Methylene blue (MB) and Rhodamine B (RhB) under visible light.

11p viengfa 28-10-2024 1 0   Download

In this work, ZnFe2O4 nanoparticles were synthesized by hydrothermal method while the hummer method was used to synthesize GO nanosheet. GO/ZnFe2O4 nanocomposites (GO/ZFO) were prepared by mixing GO with ZnFe2O4 in mass ratio of 1:99, respectively.

8p viengfa 28-10-2024 2 1   Download

In the present work, CeO2 with different loading was embedded on reduced graphene oxide (rGO) by a simple one-pot hydrothermal method. The synthesized samples were characterized using XRD, EDX mapping, FESEM, and UV-Vis DRS techniques.

11p vifilm 11-10-2024 2 0   Download

In this research, the nanosized Fe2V4O13 complex oxide material was synthesized by the hydrothermal method. Its structure, morphology characterization, and other properties were determined using X-ray, SEM, EDX, and DTA-TG methods.

5p vikwong 29-09-2024 2 1   Download

Zeolite, as chemical essence, is an aluminosilicate mineral synthesized by richsilica source, such as rice husk ash (RHA). This study focuses on the synthesis of zeolite NaP1 under a facial hydrothermal method using the silica source utilized from RHA without any-pretreatment steps.

6p vikwong 29-09-2024 2 1   Download

In this study, γ-MnOOH nanorods synthesized by polysaccharide- assisted hydrothermal method as an efficient electrocatalyst for urea oxidation. The γMnOOH structure and morphology are confirmed by X-ray diffraction and scanning electron microscopy (SEM).

5p vikwong 29-09-2024 2 0   Download

The results showed that GdFeO3 photocatalyst had a good performance under visible light irradiation. The remarkable enhancement photo-Fenton catalytic activity of GdFeO3 material could be attributed to its small particle size and narrow band gap energy.

6p vikwong 29-09-2024 1 0   Download

The results show that the sulfur source plays a crucial role in determining the product morphology. Photocatalysis experiments show Bi2S3 nanowires exhibit the highest photocatalytic reduction of Cr(VI) when exposed to visible light irradiation.

5p vikwong 29-09-2024 3 0   Download

Novel g-C3N4/InVO4 materials were synthesized by a fabricated via hydrothermal and heating methods. The physicochemical properties of the photocatalysts were investigated by X-ray diffraction (XRD), infrared spectroscopy (IR), Photoluminescence spectroscopy (PL), UV-Vis diffuse reflectance spectroscopy (UV-Vis-DRS) and Energy dispersive X-ray spectroscopy (EDX).

5p vikwong 29-09-2024 1 0   Download

The high durability, re-collectable and low-cost materials with tertiary (reduced graphene-TiO2-Fe3O4, denoted as GrTiFe) components for degradation of toxic organic compounds have been prepared from different precursors by coprecipitation and hydrothermal methods.

5p vikwong 29-09-2024 1 0   Download

The synthesis and Rhodamine B removal efficiency of monazite monoclinic BiPO4 by hydrothermal route using Bi(NO3)3·5H2O, K2HPO4·3H2Oand HNO3 as staring materials were presented in this work. The obtained samples were characterized by X-ray powder diffraction, high-resolution transmission fieldemission scanning electron microscopy and diffuse reflectance UV-Vis spectrometry.

4p vikwong 29-09-2024 0 0   Download

In this study, the Cu-TiO2-SBA-16 photocatalytic materials were successfully prepared by direct hydrothermal synthesis method. The products were characterized by X-ray diffraction (XRD), Ultraviolet– Visible Diffuse Reflectance Spectroscopy (UV-Vis DRS), energy dispersive X-ray (EDX), transmission electron microscopy (TEM), N2 adsorption–desorption isotherms, X-ray photoelectron spectroscopy (XPS) methods.

6p vikwong 29-09-2024 2 0   Download

Zeolite seed-based mesoporous aluminosilicate material MSU-S is normally synthesized from pure chemicals. In the study, MSU-S material was synthesized using natural resources such as rice husk, and kaolin in Vietnam. Here, a systematic investigation is conducted to find the relationship between the synthesis conditions (aging time, hydrothermal time, hydrothermal temperature, pH environment) and the formation of mesoporous structure, as well as the material properties.

6p vikwong 29-09-2024 5 0   Download

CuO nanoparticles were synthesized by alcohol-assisted hydrothermal method at various pH values, using sodium hydroxide as a precursor for pH control. The chemical composition, morphological and structural properties of the obtained CuO nanoparticles were investigated by the Raman and energy-dispersive X-ray spectroscopies, the field-emission scanning electron microscopy, and the X-ray diffraction.

12p dianmotminh02 03-05-2024 3 1   Download

This article, we present a thorough and straightforward hydrothermal method towards the production of reduced graphene oxide templated MIL-53(Fe) hybrids RGO@MIL-53(Fe). The structural characteristics of created hybrids were identified by using BET, FESEM, powder X-ray diffraction, and FTIR techniques. Methylene blue (MB) dye (a model water pollutant) was used to evaluate H2O2-assisted photo-catalytic efficiency of RGO@MIL-53(Fe).

9p dianmotminh02 03-05-2024 4 2   Download

In this work, gold nanorods (AuNRs) with well-controlled aspect ratios were prepared using a modified seedgrowth method and covered by TiO2 layers through the hydrothermal reaction to improve stability. Integrating TiO2 with plasmonic rod-like gold nanoparticles could enhance their photo activity by the local surface plasmon resonance (LSPR) effect. AuNRs aspect ratios were controlled by varying the amount of seed solution, reducing agents, surfactant (CTAB), and titanium (IV) but oxide.

7p dianmotminh02 03-05-2024 9 3   Download

The results show that the cerium oxide spherical nanoparticles built from primary nanoparticles with the average size of ~5 nm, exhibited dispersion and uniform size and shapes with their average particle diameter of ~50 nm in size. With such a good morphology, CeO2 material possessed good catalytic activity for the decomposition of methylene blue (MB), in which the material was synthesized at a hydrothermal temperature of 80 oC (CeO2-80) for the best MB decomposition performance.

10p meyerowitz 25-12-2021 5 0   Download

In the present study, we have follwed the hydrothermal path for the synthesis of gold nanoparticles (Au NPs) from the biomaterial Elaeocarpus ganitrus seeds extract, which is a rapid, eco-friendly, non-chemical way. The prepared NPs were thoroughly analysed by powder x-ray diffraction and high resolution transmission electron microscopy studies and were also tested for anticancer studies.

7p meyerowitz 25-12-2021 25 1   Download

The purpose of this thesis is to study and synthesize BiMO materials (M = V,Ti,Sn) by microwaveassisted chemical method, hydrothermal method, sol-gel method and evaluate their physical properties. The synthesized materials (Bi2Sn2O7 and Bi2Ti2O7) were investigated the photocatalytic activity in the decomposition of RhotaminB (RhB) under visible light.

28p thebadguys 08-06-2021 22 3   Download

In this paper, modified hydrothermal method for Ti-MWW catalyst preparation has been shown. Instrumental analysis of the zeolite material Ti-MWW has been performed by means of UV-vis spectrometry, infrared spectrometry (IR), scanning electron microscope (SEM), X-ray diffraction (XRD), and X-ray microanalysis.

8p tocectocec 25-05-2020 3 2   Download