Thermogravimetric analysis

In this paper, polyvinyl butyral (PVB) composite coating was prepared with graphene oxide (GO) to improve mechanical properties, corrosion protection, and thermal oxidation stability. Fourier-transform infrared spectroscopy (FT-IR), Thermogravimetric analysis (TGA), Field Emission Scanning Electron Microscopy (FESEM),... were used to examine the results.

9p viambani 18-06-2024 1 0   Download

This study investigated the effect of graphene content on intumescent coating properties. Intumescent coatings contained Plextol R4152 as a binder, APP-PER-MEL as a flame retardant additive system, TiO2, Al(OH)3 as fillers, and other additive. The fire resistance test and furnace test were conducted. TGA, DSC, and SEM were used to assess the coating and char layers. The water resistance and mechanical properties of the coatings were examined.

12p dianmotminh02 03-05-2024 2 1   Download

The influence of the black seed oil modified epoxy resin (EBSO)/monomer 3,4-epoxycyclohexylmethyl 3,4- epoxycyclohexane carboxylate (BCDE) weight ratio in the coatings based on the compounds and photoinitiator triarylsulfonium hexafluoroantimonate (TAS) on thermal properties of photocrosslinked coatings have been studied. The chemical structure of investigated UV-cured coatings was characterized by IR spectrometric analysis. Their thermogravimetric (TG) and differential scanning calorimetry (DSC) behavior were determined by TG and DSC analysis, respectively.

9p dianmotminh02 03-05-2024 3 1   Download

The 3D printing PMMA/ZrO2 filaments with a diameter of 1.75±0.05 mm were fabricated by using a single-screw extruder at temperatures of four heating zones of 190, 200, 210, and 210°C. Testing samples were prepared from the extruded filaments by using a fusion deposition modeling 3D printer and a Haake MiniJet piston injection molding machine. Fourier transform infrared spectroscopy, mechanical properties, field emission scanning electron microscopy (FESEM), differential scanning calorimetry, and thermogravimetric analysis of the filaments were investigated.

9p dianmotminh02 03-05-2024 1 1   Download

The acid-treated PG was neutralized by NaOH and CO2 aeration, creating CaCO3 in situ nano-microparticles identified by scanning electron microscopy (SEM) images and CaCO3 intensity by X-ray diffraction (XRD). In this study, the cement mortar test, which used treated PG from both sulfuric treatment and NaOH neutralization within CO2 aeration, has better compressive strength properties and hydration supported by SEM images, XRD results, and thermogravimetric analysis.

8p dianmotminh02 03-05-2024 3 2   Download

Cellulose (SC) isolated from sesame seed (SS) was surface modified with the introduction of an ester functional group via a simple reaction to produce the modified product (SA). SS, SC and SA were characterized using Fourier transform infrared (FTIR), X-ray diffraction (XRD), thermogravimetric analysis (TG), particle size distribution (PSD), zeta potential and scanning electron microscopy (SEM).

7p viberbers 09-08-2023 4 3   Download

This research aimed to extract lignin from rice straw and reveal the pH value of diluted acid at which the most effective yield of lignin was precipitated. In this study, rice straw obtained from local fields in the An Giang province of Vietnam and sodium hydroxide 2 M was employed to extract lignin from rice straw.

5p vimalfoy 08-02-2023 8 2   Download

A biocompatible nanocarrier system was prepared in this research through the reaction of calcium alginate (CA) with chitosan (CS). The structure of developed nanocarriers (CS-CA) was characterized by thermogravimetric analysis (TGA), Fourier transforms infrared (FT-IR) spectroscopy, field emission scanning electron microscopy (FE-SEM), X-ray diffraction (XRD) atomic force microscopy (AFM), and transmission electron microscopy (TEM).

12p lyhuyenthu 31-01-2023 3 2   Download

In this study, cellulose acetate (CA)/polyvinylpyrrolidone (PVP) and CA/PVP/Mn2+ nanofibers were produced by the electrospinning method, and these cellulose-derived membranes were used as carriers for arginase immobilization for the first time. The structural and morphological analysis of these cellulose-derived nanofibers were determined by attenuated total reflection-Fourier to transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), X-ray diffraction (XRD), and scanning electron microscopy (SEM).

12p lyhuyenthu 31-01-2023 5 2   Download

The identification of the defects and secondary phases which significantly affect the material properties are of crucial importance. In this study, a systematic structure examination of PbTiO3 and cobalt doped PbTiO3 powder ceramics was carried out. X-ray diffraction (XRD), Fourier-transform infrared (FT-IR), Raman, and electron paramagnetic resonance (EPR) spectroscopies were applied along with nonsimultaneous thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC).

9p lyhuyenthu 31-01-2023 8 2   Download

Zirconium-2,6-naphthalenedicarboxylate metal-organic framework (Zr-NDC MOF) was prepared using ultrasound-assisted synthesis and tested for the adsorptive removal of crystal violet (CV) dye from aqueous solution. The pristine Zr-NDC was characterized using powder X-ray diffraction, scanning electron microscopy, thermogravimetric analysis, and energy-dispersive X-ray spectroscopy, Fourier-transform infrared, elemental analysis, and dynamic light scattering techniques.

12p lyhuyenthu 31-01-2023 4 1   Download

Bacterial cellulose (BC) and silk fibroin (SF) are natural biopolymers successfully applied in tissue engineering and biomedical fields. In this work nanocomposites based on BC and SF were prepared and characterized by scanning electron microscopy (SEM), infrared spectroscopy (FT-IR), X-ray diffraction (XRD) and thermogravimetric analysis (TGA).

11p vihermione 06-01-2023 5 2   Download

A polyelectrolyte complex (PEC) matrix formed between chitosan and pectin was developed to entrap a bioactive compound (anthocyanin), obtaining an useful pH indicator device. Polysaccharides of opposite charges such as chitosan and pectin can have a very strong intermolecular interaction.

9p vihermione 06-01-2023 6 2   Download

This work reports on water desorption from cassava starch in relation with the structure and conditioning of granules in suspensions or after equilibration in desiccators. The experimental work is performed by thermogravimetric analysis with isothermal and non-isothermal protocols and interpreted to derive the activation energies and desorption frequencies according to the humidity range with no adjustable parameter.

9p vihermione 06-01-2023 6 2   Download

The preparation of cellulose laurate was investigated through transesterification in 1-allyl-3- methylimidazolium chloride (AmimCl)/dimethyl sulfoxide (DMSO) cosolvent system by using vinyl laurate as an acylation reagent and 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) as an effective catalyst.

8p vihermione 06-01-2023 4 2   Download

This study investigates the effect on structural, thermal and electrical properties of PM-355 as a function of different Proton fluence values having energy of 5 MeV. The reference and irradiated samples were studied using X-ray diffraction (XRD), thermogravimetric analysis (TGA) and impedance spectroscopy techniques.

3p vironald 15-12-2022 9 3   Download

The thermal behaviour of bio-fillers and biofiller/polyolefin composites were studied with thermogravimetric analysis. The thermal analysis of the fillers showed rice husk has thermal resistance comparing to sawdust. In the air atmosphere, the main peak of rice husk degradation shifted to lower temperature values compared to that in nitrogen atmosphere.

5p vilexus 30-09-2022 12 2   Download

Đặc tính của sản phẩm cuối được đánh giá bằng các phương pháp phân tích hóa lý hiện đại như xác định diện tích bề mặt riêng BET (Brunauer-Emmett-Teller), kính hiển vi điện tử quét SEM (Scanning electron microscopy), kính hiển vi điện tử truyền qua HR-TEM (High-resolution Transmission Electron Microscope), phân tích nhiệt trọng trường TGA (Thermogravimetric Analysis).

5p viirenerosenfeld 26-05-2022 24 1   Download

This mini review identifies several thermogravimetric analysis (TGA)-based methods for the identification and quantification of different microplastics in both proof-of-concept studies and environmental samples, and highlights method-specific limitations associated with their application.

6p thebadguys 15-01-2022 14 0   Download

We characterize the trunk cuticle of velvet worms of the Peripatoides novaezealandiae-group (Onychophora) using SEM, TEM, Fourier transform infrared spectroscopy (FT-IR), and thermogravimetric analysis (TGA). TEM and SEM revealed a relatively uniform organization of the delicate cuticle that is covered by numerous bristled and nonbristled papillae with ribbed scales arranged in transverse rows. The cuticle consists of a very thin multilayered epicuticle of varying appearance followed by the largely fibrous procuticle.

9p dolomite36 30-12-2021 2 0   Download