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X-ray structural

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  • The N,O-bidentate ligand 2-((methylimino)methyl)pyren-1-ol (1) gives with nickel acetate in a mixed solvent of toluene and ethanol in the presence of NaOAc the nickel(II) complex 1(Ni). It was characterized by elemental analysis, IR, NMR, MS spectroscopy and single crystal Xray diffraction. With respect to the nickel atom the complex 1(Ni) adopts a distorted square planar trans-coordination geometry.

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  • The structural, morphological and optical properties of CBD deposited CdS thin films have been studied by varying the processing parameters and the Cd/S ratio of the starting precursors in order to better understand the growth conditions. The films were characterized by Xray diffraction, SEM, Raman, and photoluminescence spectroscopy. XRD patterns show that asdeposited CdS films were polycrystalline. The grain size are increasing with increasing the Cd/S ratio and/or the deposition time.

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