Catalysts preparation

In this study, perovskite BaTiO3 and SrTiO3 catalysts were prepared using the sol-gel method for oxidative coupling of methane (OCM). Characterization of catalysts was investigated by X-ray diffraction for crystal properties, physical N2 adsorption to determine specific surface area, and temperatureprogrammed techniques to examine the redox properties and acid–base strength.

6p vikwong 29-09-2024 1 1   Download

Volatile organic compounds (VOCs) are one of the environmental pollutants of concern because they contribute to polluted environmental phenomena such as photochemical smog and secondary particulate matter. The current research focuses on preparing the manganese oxide catalyst by many different methods and evaluating their activity in the toluene oxidation reaction.

6p vikwong 29-09-2024 2 1   Download

The prepared solids were analyzed by XRD, BET, EDS... Cobalt(II) ions supported-magnesium silicate catalysts expressed as effective catalysts for selective oxidation of benzyl alcohol using tert-butyl hydroperoxide as an oxidizing agent.

4p vikwong 29-09-2024 3 1   Download

In this paper, the Au doped Mn1Co9Ox was investigated for total oxidation of CO. The sol-gel method was applied to prepare this catalyst and some modern analysis methods as XRD, EPR, TPx, SEM were utilized to characterize its properties.

7p vikwong 29-09-2024 4 0   Download

he catalytic dehydration of ethanol is a potential alternative route to synthesize ethylene apart from the traditional method which depends on fossil fuels. This report successfully prepared modified ZSM-5 with mesopores using desilication methods to enhance ethanol catalytic dehydration performance and ethylene production at lower temperature.

5p vikwong 29-09-2024 3 1   Download

Titanium oxides nanotubes (TNTs) were prepared by hydrothermal method and used as nano-support for nickel nanoparticles. Indeed, nickel nanoparticles supported TNTs (Ni-TNTs) were in situ synthesized from nickel salt and TNTs by chemical reduction method using sodium borohydride (NaBH4) as reducing agent.

5p vikwong 29-09-2024 4 1   Download

WO3/Ag3VO4 photocatalyst was synthesized for benefiting the visible region of solar spectrum for degradation of antibiotic pollutant. The prepared catalyst was characterized by using scanning electron microscope (SEM), X-ray diffraction (XRD), infrared spectroscopy (IR) and energy-dispersive X-ray spectroscopy (EDX).

6p vikwong 29-09-2024 3 1   Download

In this study, SrTiO3 catalyst was prepared by sol-gel method and CuOZnO by co-precipitation for oxidative coupling of methane (OCM). The XRDresults showed a stable phase structure and high crystallinity with both samples. NH3-TPD recorded weak acid centers on SrTiO3, leading to coke formation on the impact surface. H2-TPR and O2 - TPD express the redox of CuO-ZnO, resulting in a deep oxidation product of CO2.

8p vikwong 29-09-2024 4 1   Download

We present a method to produce graphene flakes (GFs) from polyethylene terephthalate (PET) bottle wastes by the pyrolysis method using modified bentonite as a catalyst. The as-synthesized GFs are analyzed in terms of crystal phase, morphology, and surface chemistry. The synthesized GFs have a porous, thin, and leaf-like morphology with a length ranging from a few hundred nanometers to a few tens of micrometers.

6p vikwong 29-09-2024 2 1   Download

In this study, pellets of iron alumina pillared bentonite (PFeAPB) were prepared by dispersing iron ions on alumina pillared bentonite pellet. Catalyst activity and lifetime were investigated via efficiencies of Methyl Orange (MO) decolorization and Chemical Oxygen Demand (COD) removal, a typical dye type of textile wastewater. Characteristics of the PFeAPB catalyst were examined by X-ray diffraction (XRD), Brunauer–Emmett–Teller (BET) surface area, and X-ray fluorescence (XRF).

9p larachdumlanat127 02-01-2021 20 2   Download

TiO2-Graphene Oxide-Hemin (TiO2/GO/Hemin) ternary composite hybrid material was prepared by the sol-gel method and used as a heterogeneous catalyst for the photocatalytic degradation of organic contaminants. The catalytic activity of GO-TiO2-Hemin was evaluated by the degradation of Rhodamine B (RhB) under the UV-visible light irradiation and in the presence of hydrogen peroxide.

9p tamynhan4 06-09-2020 18 3   Download

In this paper, modified hydrothermal method for Ti-MWW catalyst preparation has been shown. Instrumental analysis of the zeolite material Ti-MWW has been performed by means of UV-vis spectrometry, infrared spectrometry (IR), scanning electron microscope (SEM), X-ray diffraction (XRD), and X-ray microanalysis.

8p tocectocec 25-05-2020 3 2   Download

Aripiprazole is a widely used antipsychotic approved by the FDA (Food and Drug Administration) in 2002. Methods for preparation of aripiprazole mainly involve the use of expensive and toxic solvents, and the reaction time can be even several hours long.

6p tocectocec 25-05-2020 11 1   Download

In this article, magnetically nanoparticles (MNPs) of CuFe2O4 were prepared and characterized using Fourier transform infrared spectroscopy, scanning electron microscopy, X-ray diffraction and transmission electron microscopy techniques.

10p tocectocec 25-05-2020 16 0   Download

Nanostructured Au-Ceria has been known as a promising catalyst for the low-temperature water-gas shisft reaction. The catalyst prepared by coprecipitation method with the gold loading various between 2 - 3 at.% with the crystallite size of 2.9 nm has been used to study some factors that effect to catalytic activity and long-term stability of this material.

5p uocvong04 24-09-2015 40 2   Download

CuO/TiO2 catalysts for the oxidation of toluene were prepared by impregnation method from copper (II) acetate precusor. The catalysts were characterized by XRD, IR and DTA/TGA.

5p uocvong03 24-09-2015 71 2   Download

Oxidation of benzyl alcohol plays an important role in organic synthesis for the purpose of producing benzandehyde - a valuable chemical intermediates. MCM-41 is an important member of M41S mesoporous materials family. It is proved to be very potential for being used as support materials due to its high specific surface area, thermal-hydrothermal stability, etc.

5p uocvong03 24-09-2015 95 6   Download

The epoxy ester was prepared from epoxy resin DER 331 and fatty acid by esterification reaction in inert gas without catalyst. The kinetics of the esterification was investigated and the results shown that the temperature, reaction time and mol ratio of epoxy resin to fatty acid suitable to electro-deposition process are 220o C, 150 minutes and 1/4, respectively. The received epoxy ester was modified with 15% (wt%) maleic anhydride at 175o C for 120 min which was adapt to binder for anodic electro-deposition coating.

5p uocvong03 24-09-2015 51 5   Download

In the Pt/
-Al2O3 catalysts, the distribution of uniform, small particle-size Pt metal on the carrier with high surface area of metal will result in high catalytic activities and will economize noble metals. The distribution of metal depends on the technology of preparation and postpreparation. The influences of the impregnating, drying, calcining and reducing on the distribution of metal have been studied using by physic methods, scan electronic microscope (SEM), transmission electronic microscope (TEM), and the hydrogen distribution has been measured by the method of hydrogen absorption.

5p uocvong01 24-09-2015 55 6   Download

Activated carbon (AC) from coconut shells is used as support for platinum catalysts. A series of catalysts based on platinum and Pt doped Sn were prepared by impregnation on different supports like AC and SiO2. It was shown that the nature of the support has a significant influence on the activity and selectivity to alkenes of the catalysts in the dehydrogenation of nhexane to alkenes. The higher activity and selectivity of the carbon supported platinum catalyst can be explained by higher dispersion of platinum particles of the catalysts.

5p uocvong01 24-09-2015 49 4   Download