Optimal pH

In this study, the objective was to employ experimental design in order to optimize the efficiency of diesel oil removal from water using activated carbon sourced from rambutan peel. A central composite design was utilized to investigate the impact of contact time, adsorbent dosage, initial oil concentration, and pH on both the removal efficiency and oil adsorption capacity across 30 different experimental designs.

12p vijaychest 24-04-2024 6 2   Download

Bài viết trình bày xác định các thông số tối ưu cho quá trình chiết xuất protein từ bã sữa gạo đã làm sạch tinh bột và carbohydrate bằng enzyme protease thương phẩm Phƣơng pháp: Nghiên cứu được thực hiện trên cơ sở khảo sát lựa chọn 9 loại enzyme thương phẩm của công ty Amano-Nhật Bản để tiến hành tối ưu hóa điều kiện enyzme hóa nhằm chiết xuất protein từ bã sữa gạo bằng phương pháp thiết kế bề mặt RSM, mô hình I-optimal. Sản phẩm của nghiên cứu được phân tích SDS-PAGE để đánh giá thành phần protein.

13p vilarry 01-04-2024 8 2   Download

In this study, the culture medium and fermentation modes were studied aiming to improve the cell density of Bacillus clausii HH1. Firstly, the factorial design method using Minimum Run Resolution IV design was used to evaluate the relative importance of culture medium components to the growth of Bacillus clausii.

9p vialfrednobel 21-12-2023 7 2   Download

The silver nanoparticles are synthesized by the green method using Salix semi-solid extract. Fresh leaves are prepared in a semi-solid extract form that retains active substances and can be preserved for a long time. The parameters of the synthesis process are optimized by examining the effects of pH, Salix semi-solid extract concentrations of extract and AgNO3 concentrations through the UV-Vis absorption spectrum of synthetic particulate solutions.

8p giangnhanly 02-10-2023 6 2   Download

In this paper, the aim was to evaluate the feasibility of a pellet reactor to treat the plating wastewater. The hydraulic retention time, the initial pH and molar ratio of carbonate to heavy metal was investigated to optimize the heavy metal removal efficiency in the pellet reactor.

6p vidoctorstrange 06-05-2023 8 4   Download

This study proceeded to address the following objectives: To evaluate the effect of gas composition commonly used in modified atmosphere packaging (80% O2 and 20% CO2) on the shelf life of beef patties; to formulate an optimal solution containing natural antioxidant and antimicrobial preservatives and to study the effect of this combination and MAP on physiochemical attributes (surface colour (chroma, hue angle), metmyoglobin and oxmyoglobin contents, lipid stability) of fresh beef patties; to evaluate the effect of combined antioxidant – antimicrobial natural preservative and MAP on packag...

95p runthenight04 02-02-2023 1 1   Download

The applicability of capillary zone electrophoresis (CZE) for the separation of the deamidated forms of insulin has been studied. 50 mM NH4Ac (pH=9) with 20 % v/v isopropylalcohol was found optimal for efficient separation of insulin from its even 10 deamidated forms.

8p viginny 23-12-2022 6 3   Download

Two mixtures of neutral cyclodextrins (CDs) were used in Electrokinetic Chromatography (EKC) to model and optimize the simultaneous enantiomeric separation of a group of seven drugs. Heptakis(2,6-di-Omethyl)-β-CD (DM-β-CD) combined with methyl-γ -CD (M-γ -CD) or with carboxyethyl-γ -CD (CE-γ -CD) was employed in a 25 mM formate buffer at pH 3.0 to have the drugs studied positively charged.

12p vironald 15-12-2022 12 2   Download

A method has been developed for the quantitative determination in cork bark macerates of 7 halophenols and 5 haloanisoles with demonstrated or suspected contribution to the cork taint off-flavour. Macerates were extracted with stirbar (20 mm polydimethylsiloxane-coated) sorptive extraction under optimized conditions (pH 3.5, 20% NaCl and 60 min).

8p vironald 15-12-2022 10 2   Download

This study presents the process of synthesizing BiFeO3 by the Gel – Polymer combustion method under optimal condition, selected through the investigation of influencing factors and the characteristic of materials, including the Gel formation temperature (80°C), the molar ratio of Bi/Fe (1/1), the molar ratio of the mixture metal/PVA (1/3), pH=1, and the sample is heated at 500oC for 2 hours.

9p viindranooyi 07-05-2022 19 1   Download

The crude enzyme extract of the strain was also characterized the activity with respect to temperature, pH, incubation period and two different enzyme substrates. High protease activity produced by Bacillus sp. B9 was observed at 36h of incubation at 45 oC with the initial pH of 9.0 by using gelatin as its substrate. Additionally, when using gelatin substrate, the protease activity was much higher than in the case of casein.

11p thebadguys 15-01-2022 13 0   Download

Disposable sensors based on a pencil graphite electrode were described for detection of alkyl phenols. The performances of the disposable bare pencil graphite electrode (PGE) and PGE modified with carbon nanotubes, regarding the cyclic and differential pulse voltammetric determination of 4-nonylphenol, 4-octylphenol, and 4-tert-octylphenol, were compared. Some experimental variables of the electrode surface pretreatment and measurement parameters were optimized. Using a phosphate buffer solution (pH 7.

10p langthannam 29-12-2021 13 0   Download

New superabsorbent hydrogels were synthesized through free radical graft copolymerization of partially neutralized acrylic acid (AA) and 2-acrylamido-2-methylpropanesulfonic acid (AMPS) onto carboxymethyl cellulose (CMC) backbones. The structure and morphology of the synthesized superabsorbent hydrogels were characterized by Fourier transform infrared spectroscopy and scanning electron microscope. The effect of the molar ratio of AMPS to AA, the APS concentration, and the CMC content on swelling ratio was optimized.

11p langthannam 29-12-2021 8 0   Download

A new, rapid, and sensitive gas chromatography–mass spectrometry (GC-MS) method was developed for the determination of ezetimibe (EZE) in human plasma. EZE was derivatized prior to GC-MS analysis. Various derivatization techniques such as acetylation, methylation, and silylation were tried. EZE was extracted from plasma with high recovery (94.39%–97.57%) using methyl tertbutyl ether and carbonate buffer (pH 9). Chromatographic conditions were optimized using chemometric methods.

12p langthannam 29-12-2021 10 0   Download

Optimization of the LiFePO4 cathode active material synthesis process in the hydrothermal method consists of many factors, including pH, carbon coating, particle size optimization, sintering and hydrothermal synthesis temperature. The main goal of this study is to determine the effect of particle size, pH and carbon coating on capacity and cycle performance. In this study, LiFePO4 cathode active materials were prepared at different pH (6.5 and 8.5) and temperature (160 and 180◦C) levels using the hydrothermal method.

12p langthannam 29-12-2021 18 1   Download

Decolorization of Reactive Red 3 from aqueous solution by laccase immobilized on the nanocomposite was studied in different conditions (pH, temperature, dye concentration, and reaction time) to investigate the decolorization activity with repeated use and storage. The results indicated that more than 77% of the activity of laccase immobilized systems was retained at the end of 10 cycles. The final decolorization capacity of the immobilized laccase was significantly higher (65%) than that of free laccase (33%) in the chosen optimized conditions (pH 5, 20 ◦ C, 0.

15p langthannam 29-12-2021 10 0   Download

In the present study, ZnO nanostructures were ultrasonically synthesized and immobilized on the surface of diatomite and used for visible light photocatalysis of Acid Red 88 (AR88) in the aqueous phase. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) analyses were employed for characterization of the samples. The process was optimized via response surface methodology (RSM) on the basis of central composite design (CCD).

13p langthannam 29-12-2021 8 0   Download

A fluorescent probe based on benzoyl hydrazine was synthesized and characterized as an Al3+-selective fluorescent probe. This probe showed good selectivity towards Al 3+ compared to other common ions. Under optimized experimental conditions, the probe exhibited a linear dynamic response for Al 3+ from 5.0 × 10−7 to 4.5 × 10−6 M with a detection limit of 1.3 × 10−7 M in ethanol–water solution (9:1, v:v, pH 6.8, 20 mM HEPES). Furthermore, it was used for imaging of Al3+ in living cells with satisfying results.

9p langthannam 29-12-2021 6 0   Download

A novel preconcentration method for Pb and Zn ions using a column packed with Schiff base modified silica gel is described. The method was based on the sorption of analytes on N,N’-bis(4-methoxysalicylidene)-1,3-propanediamine modified silica gel and elution with HNO3 prior to flame atomic absorption analysis. The parameters pH, flow rate, sample volume, eluent volume, and concentration were optimized using a central composite design.

12p langthannam 29-12-2021 10 0   Download

A novel method for the determination of mercury(II) is suggested. The procedure is based on the formation of an ion associate between the bromide complex of Hg(II) and Astrazon Red 6B dye and vortex-assisted liquid–liquid microextraction of the ion associate formed, with subsequent spectrophotometric detection. The variables that affect the procedure, such as pH, the concentration of ligand and dye, the type and volume of extraction solvent, and the rate and time of vortex mixing, were optimized.

9p langthannam 29-12-2021 7 0   Download