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Co-precipitation
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According to the batch experiments, the adsorption isotherms and the adsorption kinetics for these mesoporous materials are well fitted with the nonlinear Langmuir model and the nonlinear pseudo-second-order model, respectively. Among them, CuFe2O4 powder showed the best phosphate adsorption performance with the maximum P adsorption capacity of 27.49 mgP g-1 , which can be assigned to the highest surface area and the high pH value at its point of zero charge.
7p
dianmotminh02
03-05-2024
5
1
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The highest luminescence product consists of spheroidal and relatively uniform particles with sizes around 0.6-1.0 µm. The variation of the precipitated precursor with temperature, the influence of sintering temperature on structure and luminescence, the mineralization role of boric acid and the chemical reactions that occur with generation of precipitated precursors and upon heating to give luminescent solid solution products are mentioned.
10p
dianmotminh02
03-05-2024
2
1
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In this study, a straightforward process was employed to synthesize Fe3O4 nanoparticlesdecorated porous carbon derived from rice husk waste (Fe3O4/C). The composite material was made by using pyrolysis and then coprecipitation.
13p
viohoyo
25-04-2024
4
2
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The heterogeneous recyclable catalyst, Cu-Fe hydrotalcite, was synthesized by coprecipitation, activated at 200oC and then successfully applied in Aldol reaction. This procedure also exhibited efficiency in the total synthesis of Abhexone, a flavor with high demand in the food and cosmetic industry.
9p
viengels
25-08-2023
6
3
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Magnetic spinel ferrite nanoparticles Fe2Fe1-xMnxO4 were synthesized by a simple coprecipitation method. The morphology and structures of the synthesized samples were characterized by X-ray diffraction (XRD), field-emission scanning electron microscope (FESEM), Raman spectroscopy, and infrared spectroscopy (FTIR).
17p
viannee
02-08-2023
7
3
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The particle size, morphology and magnetic properties of CFO depend on the synthesized method. In this paper, we report the synthesis of CFO NPs by co-precipitation method and hydrothermal method at different concentration of sodium hydroxide and treatment temperatures to control size particles and magnetic properties by simple way.
6p
vidoctorstrange
06-05-2023
4
2
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Herein, a performance analysis of La-doped copper-based catalysts (CuO/ZrO2 /La-Al2 O3 ) in methanol steam reforming (MSR) was conducted and compared with a commercial low temperature water-gas shift catalyst (HiFUEL W220) to produce H2 with low CO selectivity. The physicochemical properties of as-obtained catalysts were characterized by N2 adsorption, XRD, and ICP-OES. Effect of calcination temperature (750 ℃ and 1000 ℃) on the properties of mixed oxide support (La-Al2 O3 ) were discussed based on catalytic activity.
12p
lyhuyenthu
31-01-2023
5
2
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Photocatalytic degradation of paracetamol by semiconductor oxides under UV and sunlight illumination
In this study, photocatalytic degradation of paracetamol (acetaminophen), an analgesic and antipyretic drug, was investigated in using semiconductors under UV-B and sunlight irradiation. Semiconductor materials, Bi2 O3 , ZnO, TiO2 , and ZrO2 , were prepared using simple sol–gel, coprecipitation, and microwave synthesis methods. These photocatalyts were characterized by various spectroscopic and other techniques.
9p
lyhuyenthu
31-01-2023
9
2
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Magnetic nanoparticles of Fe3O4 coated with polyaniline have been synthesised through chemical coprecipitation, and successfully characterised using different techniques such as FT-IR and X-ray diffraction. Such nanocomposite was applied as sorbent for a new magnetic micro-dispersive solid phase extraction procedure for the extraction of seven plastic migrants in jelly samples.
10p
viginny
23-12-2022
4
3
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A new method based on the combination of carrier element-free coprecipitation and flame atomic absorption spectrometric determination has been investigated for simultaneous separation and preconcentration of Pb(II) and Cu(II) ions in some environmental solid and liquid samples. The 2-{3-(4-methylbenzyl)-4-[2-(1H-indol-3-yl)ethyl]-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl}-N’-(phenylmethylene) acetohydrazide (MITA) was utilized as an organic coprecipitating agent without using a carrier element for coprecipitation of the analyte ions.
10p
langthannam
29-12-2021
8
0
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In this study, we report a simple and economic one-pot synthesis of magnetite (Fe3O4) nanostructure and its modification with tetraethyl orthosilicate by coprecipitation method. The synthesized (Fe3O4@SiO2 ) nano sorbent was applied for enhanced adsorptive removal of methylene blue by ultrasonic wave driven batch experiments. After successful synthesis, the nanostructure was characterized for their physical structure by FT-IR, VSM, TEM, and XRD. For the maximum adsorptive performance of nano sorbent, various parameters were optimized, such as dose, pH, time, concentration, and temperature.
11p
tudichquannguyet
29-11-2021
10
1
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Fe2O3 -V2O5 mixed oxides were synthesized with solid-state dispersion (SSD) and coprecipitation methods. In addition, transition metal oxides such as CuO, NiO, and Co3O4 were successfully loaded on the synthesized catalyst (Fe2O3 -V2O5) using the SSD method. The composite catalysts were inspected for their photocatalytic activities in degrading 2,4-dichlorophenol under UV light enforcement.
14p
tudichquannguyet
29-11-2021
7
1
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Magnetic and nonmagnetic activated carbons (ACs) were successfully prepared by using AC obtained from spent coffee grounds (SCGs) for use in CO2 and CH4 capture. SCGs were activated by chemical activation to produce ACs and a magnetic α-Fe2O3/AC composite was prepared by coprecipitation method from the ACs produced. Magnetic and nonmagnetic samples were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and energy dispersive X-ray spectrometry (EDX) techniques.
18p
tudichquannguyet
29-11-2021
10
1
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CuxMg1.xFe2O4 nanoparticles were successfully synthesized by coprecipitation. The samples were calcined at 900 oC for 3 h and X-ray diffraction analysis showed that Cu0.5Mg0.5Fe2O4 had a single phase cubic spinel structure, while formation of secondary phase of Fe2O3 was observed in XRD patterns of CuFe2O4, MgFe2O4. The saturation magnetization (Ms) of Cu0.5Mg0.5Fe2O4 is in between the saturation magnetization values of CuFe2O4 and MgFe2O4 nanoparticles, CuFe2O4 is a ferromagnetic material, while MgFe2O4 and Cu0.5Mg0.5Fe2O4 show superparamagnetic behavior.
9p
nguaconbaynhay12
13-06-2021
24
1
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Lanthanum orthoferrite (LaFeO3 ) photocatalysts were synthesized by a facile and cost-effective coprecipitation method via the hydrolysis of La (III) and Fe (III). The characteristics of LaFeO3 were investigated through thermogravimetric analysis (TGA), X-ray diffraction (XRD), UV-Vis diffuse reflectance spectroscopy (DRS), vibrating sample magnetometry (VSM), and transmission electron microscopy (TEM).
7p
kethamoi7
15-08-2020
16
2
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This study describes a preparation of magnetite nanoparticle by co-precipitation of Fe(II) and Fe(III) in alginate hydrogel matrix. This simple process is sufficient for producing a superparamagnetic, well dispersible magnetite nanoparticle in polymer hydrogel matrix. Two approaches for iron ions loadings are induced. The first approach includes two steps, the hydrogel beads are formed before the iron ions are being diffused into the hydrogel matrix. The second approach is the simultaneous forming of hydrogel containing iron ions.
7p
abcxyz123_02
03-03-2020
11
1
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Contributions of the phases in the coated samples as well as structural parameters were determined from XRD data using Rietveld refinement analysis. Magnetization of the core can be improved by adjusting the modification steps. XRD analysis result and SEM images revealed the formation of core/shell structure in the sample coated by using coprecipitation method.
9p
cathydoll4
21-02-2019
27
0
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Mg0.6Al0.4(OH)2(MoO4)0.2.mH2O was prepared via coprecipitation method and characterized by XRD, BET, EDS techniques. The solid has a hydrotalcite-like structure and molybdate anions stayed in the interlayer regions between two brucite sheets. The synthesized material has been used as heterogeneous catalyst for the liquid oxidation of styrene with air. The oxidation reaction was carried out at atmospheric pressure in the temperature range of 60-110 oC.
5p
giesumanh
04-11-2018
57
0
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Nanostructured Au-Ceria has been known as a promising catalyst for the low-temperature water-gas shisft reaction. The catalyst prepared by coprecipitation method with the gold loading various between 2 - 3 at.% with the crystallite size of 2.9 nm has been used to study some factors that effect to catalytic activity and long-term stability of this material.
5p
uocvong04
24-09-2015
38
2
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This study reports the identification and characterization of the regulatory subunit, TbRSU, of protein kinase A of the parasitic protozoon Trypanosoma brucei. TbRSU is coded for by a single copy gene. The protein contains an unusually long N-terminal domain, the pseudosubstrate site involved in binding and inactivation of the catalytic subunit, and two C-terminally located, closely spaced cyclic nucleotide binding domains.
10p
system191
01-06-2013
33
3
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