Chromatography

Thin layer chromatography and column chromatography were performed from the ethyl acetate extraction of the bark stem of Phyllanthus acidus, and six terpenoids were isolated, including four diterpenes and two triterpenes. Their names were phyllanthol (1), 19-acetoxy-16α, 17- dihydroxy-ent-kaurane (2), 16α, 17-dihydroxy-ent-kaurane (3), 16α,17-acetonide-3αhydroxykauran (4), maslinic acid (5) and phyllane A (6).

8p viaburame 14-03-2025 0 0   Download

Ocimum africanum L. is a distinctive Vietnamese herb, especially common in Tuy Hòa, Phú Yên. This study focuses on extracting and analyzing the chemical composition of the essential oil derived from the leaves of Ocimum africanum. The essential oil was extracted using the steam distillation method and its chemical composition was analyzed using gas chromatography-mass spectrometry (GC-MS).

7p viaburame 14-03-2025 2 0   Download

Red yeast rice is produced from rice using Monascus purpureus fungus, which results in the red colour of the fermented rice. Red yeast rice has been used for a thousand years as a food preservative and in traditional medicine to support vascular and digestive health. This study used Liquid Chromatography-Mass Spectrometry (LC-MS/MS) to concurrently analyse citrinin and monacolin K produced by M. purpureus strain.

11p viaburame 14-03-2025 1 1   Download

In this report, the solid phase extraction technique combined with the gas chromatographymass spectrometry method (GC-MS) was optimized to determine the contamination of nine phthalic acid esters (PAEs) in the surface sediment samples collected from Rao Cai River in Ha Tinh, Vietnam.

7p vifilm 11-10-2024 1 1   Download

This study aimed to validate a procedure for the quantification of verbascoside in the root of Rehmannia glutinosa varieties 19 by high performance liquid chromatography (HPLC) to serve the assessment of medicinal quality

8p viyoko 01-10-2024 6 1   Download

Acetylcholinesterase (AChE) has been one of the important and potential targets in the discovery, and development of new drugs for treating and slowing the progression of Alzheimer's disease (AD). This research suggests potential structural frameworks for synthesizing AChE inhibitor derivatives for treating AD.

11p vihyuga 04-03-2025 1 1   Download

Octylmethoxycinnamate (OMC), octylsalicylate (OS) are UV filters commonly used in sunscreen creams for skin protection against UV radiations. In this study, an HPTLC method was developed and validated for simultaneous determination of OMC and OS in sunscreen creams.

11p vihyuga 04-03-2025 1 0   Download

Carvedilol is a pharmaceutical substance listed in the “Regulatory requirements of bioequivalence study reports for generic drugs containing APIs upon applying for marketing authorization”. Therefore, a simple method for quantifying carvedilol in human plasma is desirable.

6p vihatake 06-01-2025 3 2   Download

The combination of hydrochlorothiazide (HCT), amlodipine besylate (AML) and olmesartan medoxomil (OLM) is highly effective in treating hypertension. Currently, Vietnamese Pharmacopoeia V and other reference pharmacopoeias do not have a procedure for the simultaneous quantification of these three ingredients. To develop and validate a procedure for simultaneous determination of HCT, AML and OLM in tablets by HPLC method.

11p viharuno 03-01-2025 5 2   Download

Cajuput oil is a traditional and famous product of Thua Thien Hue, it is considered as a potential product, contributing to the economic development of Thua Thien Hue. Currently, there are many different products of cajuput oil in the market.

4p viuchiha 03-01-2025 4 2   Download

Objectives: (1) Developing a capillary zone electrophoresis method for determining simultaneously paracetamol and diclofenac in pharmaceutical formulations (2) Applying this method on the products circulated on the market. Materials and methods: Paracetamol and diclofenac in Zengesic and Ripaigesic film-coated tablets were used in this research.

7p viuchiha 03-01-2025 3 2   Download

HPLC là chữ viết tắt của 04 chữ cái đầu bằng tiếng Anh của phương pháp sắc ký lỏng hiệu năng cao ( High Performance Liquid Chromatography) ,trước kia gọi là phương pháp sắc ký lỏng cao áp (High Pressure Liquid Chromatography) ,trước kia gọi là phương pháp sắc ký lỏng cao áp (High Pressure Liquid Chrom atography) Phương pháp này ra đời từ năm 19671968 trên cơ sở phát triển và cải tiến từ phương pháp sắc ký cột cổ điển . Hiện nay phương pháp HPLC ngày càng phát triển và hiện đại hoá cao nhờ sự phát triển nhanh chóng của ngành chế tạo m...

50p nguyenvanquy1607 19-06-2010 2126 734   Download

Is a branch of polymer science dealing with analysis and characterisation of polymers. üThe complication of macromolecular chains, the dispersion in molecular weight, tacticity, crystallinity, orientation, composition of polymers etc. and complex morphological systems ⇒ analysis of polymer ≠ the small organic materials ⇒ Focus on viscoelastic properties, dynamic mechanical testing.

114p buitiendung87 06-01-2011 347 154   Download

Sắc ký (Chromatography) là phương pháp tách, phân ly, phân tách các chất dựa vào sự phân bố khác nhau của chúng giữa hai pha động và tĩnh. Khi tiếp xúc với pha tĩnh, các cấu tử của hỗn hợp sẽ phân bố giữa pha động và pha tĩnh tương ứng với tính chất của chúng (tính bị hấp phụ, tính tan, …). Trong hệ thống sắc ký chỉ có các phân tử pha động mới chuyển động dọc theo hệ sắc ký. Các chất khác nhau sẽ có ái lực khác nhau với pha động và pha tĩnh. Trong quá...

71p anhthaopro 15-04-2011 1259 410   Download

Sắc ký lỏng hiệu năng cao là một phương pháp chia tách trong đó pha động là chât lỏng và pha tĩnh chứa trong cột là chất rắn đã được phân chia dưới dạng tiểu phân hoặc một chất lỏng phủ lên một chất mang rắn ,hay một chất mang đã được biến đổi bằng liên kết hoá học với các nhóm chức hữu cơ .Quá trình sắc ký lỏng dựa trên cơ chế hấp phụ,phân bố ,trao đổi Ion hay phân loại theo kích cỡ ( Rây phân tử ) ....

50p vtanguyet88tv 10-01-2013 695 103   Download

Bài giảng Phương pháp phân tích hiện đại - Chương 20: Một số phương pháp phân tích sắc ký (Phần 2) có nội dung trình bày về sắc ký khí GC (Gas Chromatography); nguyên tắc, hệ sắc ký khí, kỹ thuật thực nghiệm và ứng dụng sắc ký khí GC,... Mời các bạn cùng tham khảo chi tiết nội dung bài giảng!

58p bachtudu 10-11-2021 37 3   Download

The study clarified the main chemical composition of the roots of F. multiflora. Studying and developing a process of qualitative and quantitative analysis of several active ingredients at the same time. Application of analytical procedure has established and evaluated the content of active ingredients in some F. multiflora medicinal samples. The research results are obtained as a scientific basis for further studies.

23p extraenglish 24-05-2021 28 2   Download

The objects of the thesis: Study and develop the simultaneous analysis method of plant growth stimulants in vegetables using by high-performance liquid chromatography coupled with ion-trapping mass spectrometry. Apply the studied method of analysis and assessment of the current use, residue level and the potential accumulation of plant growth stimulants used in vegetable production in several districts belonged to Hanoi.

28p extraenglish 24-05-2021 19 3   Download

A simple and inexpensive method was developed using liquid - liquid extraction, together with high performance chromatographic method for determination of methoxyfenozide residues in grapes. The evaluated parameters include the extracts by distilled water and acetonitrile solvents. The method was validated using grapes samples spiked with methoxyfenozide at different fortification levels (0.05, 0.1 and 0.5 µg/g). Average recoveries (using each concentration three replicates) ranged 86-95 %, with relative standard deviations less than 5%, calibration solutions concentration in the range 0.

8p chauchaungayxua6 26-06-2020 16 2   Download

In this study, behaviors of gas inside the extraction chromatography column were investigated through experiments and Computation Fluid Dynamics (CFD) simulation. N2 gas once accumulated as bubbles in the packed bed was hardly discharged by the flow of mobile phase.

8p christabelhuynh 31-05-2020 16 2   Download